Heat resistance under load: HDT, Tg, annealing and service temperature
Read thermal measurements by their method, stress and material state before selecting a hot fixture, housing or tool. An HT-PLA example shows why annealing and load belong beside the temperature.
A thermal number needs a load, a duration and a process
Engineering interpretation. Start with the temperature at the loaded feature and the permitted dimensional drift. HDT is useful screening evidence when its stress, method and material state are attached. It does not certify how long a printed housing, fixture or tool will hold its shape in service. Tg, Vicat and a no-load heat-stability claim answer different questions. ISO [details] · ASTM International [details]
The example below keeps one commercial grade’s as-printed and annealed HDT results separate at two test stresses. It illustrates how to read a sheet, rather than ranking PLA, PETG, ASA and PC from unrelated thermal numbers. ISO [details] · Polymaker [details]
One grade, two stresses, two thermal states
Polymaker labels these HT-PLA results as printed or annealed. The sheet does not identify HDT-specific orientation, geometry, heating rate, conditioning or specimen count. Unknowns remain visible in each test record; the listed values are supplier typical results, not component design limits. Polymaker [details] · ISO [details]
Engineering interpretation. Read the stresses as separate tests. The annealed result at the lower stress cannot replace the higher-stress result when screening a loaded feature. Neither is a safe operating temperature for an arbitrary geometry. Polymaker [details] · Polymaker [details] · ISO [details]
HT-PLA at 0.45 MPa
Supplier ISO 75 results at 0.45 MPa. Same commercial grade; separate thermal states. HDT orientation, geometry, conditioning, heating rate and annealing test schedule are not reported.
| Exact grade & process | Orientation & specimen state | HDT at 0.45 MPa °C | Test conditions & source |
|---|---|---|---|
| Polymaker HT-PLAFFF · Manufacturer test | Not reportedConditioning: Not reportedPost-processing: As printed (source label) | 61.4 Polymaker [details] | ISO 75 (part and revision not reported)Test temperature: Not reportedStress: 0.45 MPaDuration: Not reportedHumidity: Not reportedAnnealing schedule: Not reportedHeating rate: Not reportedSpecimen & processing details |
| Polymaker HT-PLAFFF · Manufacturer test | Not reportedConditioning: Not reportedPost-processing: Annealed; exact test-specimen schedule not identified | 107.2 Polymaker [details] | ISO 75 (part and revision not reported)Test temperature: Not reportedStress: 0.45 MPaDuration: Not reportedHumidity: Not reportedAnnealing schedule: Not reportedHeating rate: Not reportedSpecimen & processing details |
Do not substitute a different stress, post-processing state or test method. These values do not establish a continuous-use temperature. ISO [details] · ISO [details]
HT-PLA at 1.8 MPa
Supplier ISO 75 results at 1.8 MPa. Same commercial grade; separate thermal states. HDT orientation, geometry, conditioning, heating rate and annealing test schedule are not reported.
| Exact grade & process | Orientation & specimen state | HDT at 1.8 MPa °C | Test conditions & source |
|---|---|---|---|
| Polymaker HT-PLAFFF · Manufacturer test | Not reportedConditioning: Not reportedPost-processing: As printed (source label) | 58.6 Polymaker [details] | ISO 75 (part and revision not reported)Test temperature: Not reportedStress: 1.8 MPaDuration: Not reportedHumidity: Not reportedAnnealing schedule: Not reportedHeating rate: Not reportedSpecimen & processing details |
| Polymaker HT-PLAFFF · Manufacturer test | Not reportedConditioning: Not reportedPost-processing: Annealed; exact test-specimen schedule not identified | 71.7 Polymaker [details] | ISO 75 (part and revision not reported)Test temperature: Not reportedStress: 1.8 MPaDuration: Not reportedHumidity: Not reportedAnnealing schedule: Not reportedHeating rate: Not reportedSpecimen & processing details |
Do not substitute a different stress, post-processing state or test method. These values do not establish a continuous-use temperature. ISO [details] · ISO [details]
Tg, HDT and Vicat measure different responses
Engineering interpretation. A DSC Tg comes from a heat-capacity change. A DMA Tg is assigned from a change in viscoelastic response; the technique and its frequency matter. Ask which definition was used, and retain the scan rate, thermal history and conditioning when reported. Do not treat a Tg entry as a load-bearing endurance result. ASTM International [details] · ASTM International [details]
Engineering interpretation. HDT observes deflection while a loaded specimen is heated. ISO 75-2 distinguishes a 0.45 MPa stress from a 1.8 MPa stress. Vicat instead observes needle penetration. A higher Vicat value does not supply the missing HDT value for a housing wall or fixture arm. ISO [details] · ASTM International [details]
Keep ASTM D648 results outside an ISO 75 numerical comparison. The ASTM scope explicitly distinguishes their technical content. Matching the word “HDT” or rounding their stress labels does not make the methods interchangeable. ASTM International [details]
Treat annealing as a manufacturing state to qualify
Independent work by Benwood and colleagues on True Red PolyLite PLA supports a mechanism: the printing and post-print thermal history changed crystallinity and the measured heat-deflection response. That study used its own FDM process and ASTM D648 procedure. Its results and annealing recipes are kept separate from the HT-PLA supplier table. ACS Omega [details]
Engineering interpretation. For an annealed candidate, qualify the complete sequence: printing, the actual part-temperature history, support during heating, cooling and final inspection. Check critical holes, locating surfaces and assembled fit after treatment. If the annealing schedule behind a published result is unknown, request it before treating a recommendation as a reproduced test condition. Polymaker [details] · ACS Omega [details]
Use the service load to choose the next measurement
Engineering interpretation. For a hot locating fixture, measure drift at the locating surface while it carries the required force. For an electronics housing, inspect loaded standoffs, latches and fasteners after the required thermal hold and cycles. For a tool touching a hot workpiece briefly, reproduce the contact duration and cooling cycle. These examples define component checks; they are not claims that the illustrated grade has passed them. ISO [details]
Long holds need time-dependent evidence. Fischbach and Weinberg observed continuing creep in a printed Ultrafuse PLA specimen below its glass transition during a room-temperature hold. This does not predict the HT-PLA grade’s life; it shows why being below Tg alone cannot establish dimensional stability under sustained load. Fischbach and Weinberg [details]
Engineering interpretation. If the candidate lacks appropriate creep or retained-property data, test a representative part at its service temperature and environment. Include the load path and attachment points. Define allowable drift and permanent set before the test; do not invent a universal temperature margin below HDT. ISO [details] · Fischbach and Weinberg [details]
What these records establish and what remains unknown
The supplier’s “as printed” thermal labels establish a printed-material basis, but its mechanical coupon drawings do not establish the HDT orientation. General specimen instructions are also not a confirmed HDT recipe. Annealing state is known where labeled; the exact thermal-test annealing schedule remains unknown. Polymaker [details]
A similar source-boundary issue appears in the Prusament PC Blend sheet: HDT is in its typical-material table, outside the separately labeled printed-mechanical table. This article does not assign those thermal values the tensile specimen’s orientation or printing recipe. Ask the supplier for the thermal specimen process before comparing that row with confirmed printed tests. Prusa Polymers a.s. [details]
The comparison still needs HDT specimen geometry, build orientation, heating rate, conditioning and replicate information, plus sustained-load or component evidence for the proposed use. A document access date records consultation, not a fresh test. Polymaker [details] · ISO [details]
Polymaker HT-PLA · Not reported
- Material identity
- Polymaker · PLA · filler: Not reported
- Process
- FFF
- Source orientation
- Not reported
- Specimen geometry
- Not reported
- Test method
- ISO 75 (part and revision not reported)
- Test rate
- Not reported
- Test temperature
- Not reported
- Specimen conditioning
- Not reported
- Printer
- Not reported
- Post-processing
- As printed (source label)
- Sample count
- Not reported
- Meaning of ±
- Not reported
- Source locator
- PDF p. 3, Thermal Properties, data row 7, ISO 75 0.45 MPa, as printed; PDF pp. 5–6 give separate general recommendations and specimen instructions.
- Layer height
- Not reported
- Infill
- Not reported
- Perimeters
- Not reported
- Nozzle temperature
- Not reported
- Bed temperature
- Not reported
- Chamber temperature
- Not reported
- Slicer
- Not reported
- Infill print speed
- Not reported
- Top bottom solid layers
- Not reported
- Specimen cooling
- Not reported
- Extrusion multiplier
- Not reported
- Stress
- 0.45 MPa
- Thermal state
- as printed
- Duration
- Not reported
- Humidity
- Not reported
- Annealing
- As printed (source label)
- Annealing schedule
- Not reported
- Heating rate
- Not reported
- Specimen settings scope
- General specimen instructions on PDF p. 6 are not specifically assigned to HDT.
Polymaker HT-PLA · Not reported
- Material identity
- Polymaker · PLA · filler: Not reported
- Process
- FFF
- Source orientation
- Not reported
- Specimen geometry
- Not reported
- Test method
- ISO 75 (part and revision not reported)
- Test rate
- Not reported
- Test temperature
- Not reported
- Specimen conditioning
- Not reported
- Printer
- Not reported
- Post-processing
- Annealed; exact test-specimen schedule not identified
- Sample count
- Not reported
- Meaning of ±
- Not reported
- Source locator
- PDF p. 3, Thermal Properties, data row 10, ISO 75 0.45 MPa, annealed; PDF pp. 5–6 give separate general recommendations and specimen instructions.
- Layer height
- Not reported
- Infill
- Not reported
- Perimeters
- Not reported
- Nozzle temperature
- Not reported
- Bed temperature
- Not reported
- Chamber temperature
- Not reported
- Slicer
- Not reported
- Infill print speed
- Not reported
- Top bottom solid layers
- Not reported
- Specimen cooling
- Not reported
- Extrusion multiplier
- Not reported
- Stress
- 0.45 MPa
- Thermal state
- annealed
- Duration
- Not reported
- Humidity
- Not reported
- Annealing
- Annealed (source label)
- Annealing schedule
- Not reported
- Heating rate
- Not reported
- Specimen settings scope
- General specimen instructions on PDF p. 6 are not specifically assigned to HDT.
Polymaker HT-PLA · Not reported
- Material identity
- Polymaker · PLA · filler: Not reported
- Process
- FFF
- Source orientation
- Not reported
- Specimen geometry
- Not reported
- Test method
- ISO 75 (part and revision not reported)
- Test rate
- Not reported
- Test temperature
- Not reported
- Specimen conditioning
- Not reported
- Printer
- Not reported
- Post-processing
- As printed (source label)
- Sample count
- Not reported
- Meaning of ±
- Not reported
- Source locator
- PDF p. 3, Thermal Properties, data row 6, ISO 75 1.8 MPa, as printed; PDF pp. 5–6 give separate general recommendations and specimen instructions.
- Layer height
- Not reported
- Infill
- Not reported
- Perimeters
- Not reported
- Nozzle temperature
- Not reported
- Bed temperature
- Not reported
- Chamber temperature
- Not reported
- Slicer
- Not reported
- Infill print speed
- Not reported
- Top bottom solid layers
- Not reported
- Specimen cooling
- Not reported
- Extrusion multiplier
- Not reported
- Stress
- 1.8 MPa
- Thermal state
- as printed
- Duration
- Not reported
- Humidity
- Not reported
- Annealing
- As printed (source label)
- Annealing schedule
- Not reported
- Heating rate
- Not reported
- Specimen settings scope
- General specimen instructions on PDF p. 6 are not specifically assigned to HDT.
Polymaker HT-PLA · Not reported
- Material identity
- Polymaker · PLA · filler: Not reported
- Process
- FFF
- Source orientation
- Not reported
- Specimen geometry
- Not reported
- Test method
- ISO 75 (part and revision not reported)
- Test rate
- Not reported
- Test temperature
- Not reported
- Specimen conditioning
- Not reported
- Printer
- Not reported
- Post-processing
- Annealed; exact test-specimen schedule not identified
- Sample count
- Not reported
- Meaning of ±
- Not reported
- Source locator
- PDF p. 3, Thermal Properties, data row 9, ISO 75 1.8 MPa, annealed; PDF pp. 5–6 give separate general recommendations and specimen instructions.
- Layer height
- Not reported
- Infill
- Not reported
- Perimeters
- Not reported
- Nozzle temperature
- Not reported
- Bed temperature
- Not reported
- Chamber temperature
- Not reported
- Slicer
- Not reported
- Infill print speed
- Not reported
- Top bottom solid layers
- Not reported
- Specimen cooling
- Not reported
- Extrusion multiplier
- Not reported
- Stress
- 1.8 MPa
- Thermal state
- annealed
- Duration
- Not reported
- Humidity
- Not reported
- Annealing
- Annealed (source label)
- Annealing schedule
- Not reported
- Heating rate
- Not reported
- Specimen settings scope
- General specimen instructions on PDF p. 6 are not specifically assigned to HDT.
Before selecting a hot fixture, housing or tool
Engineering interpretation. Use these as project checks, with acceptance limits chosen for the actual function. A thermal label alone cannot close them. ISO [details]
Record the exact grade and lot where relevant, fabrication process, orientation and full post-processing state. Preserve the measured part-temperature history if annealed.
Check the temperature at critical loaded features, including local heat sources and the required hold or contact cycle.
Verify displacement, permanent set and fit under the actual supports, fasteners and load; repeat the relevant thermal and moisture conditions.
Where endurance matters, obtain or generate time-dependent data over the required conditions. Recheck the geometry or manufacturing route if the evidence cannot support the required margin. ISO [details] · Fischbach and Weinberg [details]
Sources and evidence records
These records distinguish supplier tests, independent experiments and engineering interpretation. “Not reported” identifies a source gap; it is not an assumed test condition.
- Prusament PC Blend technical data sheet
Prusa Polymers a.s. · Manufacturer test · document date: 2022-02-16 · version: 1.1 · accessed 2026-10-18
Prusa Polymers a.s.Manufacturer measurements on FFF coupons for this commercial product; color, lot and reinforcement content are not specified. No raw replicate data or definition of the reported plus/minus term is supplied. Printed-coupon tensile results do not report conditioning, test temperature, test rate, detailed dimensions or specimen count. The 24 °C / 22% humidity footnote belongs to the separate moisture-uptake rows and is not treated as a tensile conditioning protocol. Its polymer is described as a PC blend; the other blend constituents are not identified.
- Effect of physical aging on the flexural creep in 3D printed thermoplastic
Fischbach and Weinberg · Independent experiment · document date: 2023-08-16 · version: arXiv:2302.11240v2 · accessed 2026-10-18
Marcel Fischbach, Kerstin WeinbergAuthor manuscript, printed BASF Ultrafuse PLA; 100% infill, 0.2 mm layers, 215 °C nozzle, 30 °C bed; ISO 899-2 bending creep. The long-duration test uses one specimen under a 10 N nominal force for 170 h near 20 °C. No family-wide lifetime or reduction factor is inferred. The long-duration specimen had an initial age of five hours; the authors report laboratory relative humidity of 30–50%.
- ISO 75-1:2020 — Plastics — Determination of temperature of deflection under load — Part 1: General test method
ISO · Test method scope · document date: 2020-02-28 · version: ISO 75-1:2020, edition 4 · accessed 2026-10-18
ISOPublic abstract, not the paid full standard. Its method scope and limits explain HDT; it does not establish the edition used by the filament supplier.
- ISO 75-2:2013 — Plastics — Determination of temperature of deflection under load — Part 2: Plastics and ebonite
ISO · Test method scope · document date: Not reported · version: ISO 75-2:2013, edition 3; publication month 2013-04 · accessed 2026-10-18
ISOPublic abstract identifies the method stresses. Exact publication day was not recorded; no day is invented.
- ASTM D648-18 — Standard Test Method for Deflection Temperature of Plastics Under Flexural Load in the Edgewise Position
ASTM International · Test method scope · document date: 2018-04-23 · version: D648-18 · accessed 2026-10-18
ASTM InternationalPublic scope and significance/use explain the limits of this test and its technical differences from ISO 75. This does not certify supplier compliance.
- ASTM D1525-25 — Standard Test Method for Vicat Softening Temperature of Plastics
ASTM International · Test method scope · document date: 2025-03-04 · version: D1525-25 · accessed 2026-10-18
ASTM InternationalPublic scope identifies the controlled needle-penetration measurement. No full standard text or product-specific Vicat qualification is reproduced.
- ASTM E1356-25 — Standard Test Method for Assignment of the Glass Transition Temperatures by Differential Scanning Calorimetry
ASTM International · Test method scope · document date: 2025-01-22 · version: E1356-25 · accessed 2026-10-18
ASTM InternationalPublic scope and significance/use explain the DSC heat-capacity transition, rather than a component load-bearing limit.
- ASTM E1640-23 — Standard Test Method for Assignment of the Glass Transition Temperature By Dynamic Mechanical Analysis
ASTM International · Test method scope · document date: 2023-08-15 · version: E1640-23 · accessed 2026-10-18
ASTM InternationalPublic significance/use explains the viscoelastic transition, dependence on the measurement technique, and the ideal storage-modulus-onset interpretation.
- Polymaker HT-PLA Technical Data Sheet
Polymaker · Manufacturer test · document date: Not reported · version: V1.1 in the linked PDF filename; no printed issue date identified · accessed 2026-10-18
PolymakerPDF thermal rows explicitly separate as-printed and annealed material. HDT geometry, orientation, conditioning, replicate count, heating rate and actual annealing schedule are not identified. The general specimen recipe and recommended anneal are not silently assigned to the HDT tests.
- Improving the Impact Strength and Heat Resistance of 3D Printed Models: Structure, Property, and Processing Correlationships during Fused Deposition Modeling (FDM) of Poly(Lactic Acid)
ACS Omega · Independent experiment · document date: 2018-04-23 · version: ACS Omega 3(4), 4400–4411; DOI 10.1021/acsomega.8b00129 · accessed 2026-10-18
Claire Benwood, Andrew Anstey, Jacek Andrzejewski, Manjusri Misra, Amar K. MohantyTrue Red PolyLite PLA, 2.85 mm filament, Lulzbot Taz 6. The study combines printed and separately identified injection-molded specimens; only its printed-process observations inform this article. Its ASTM D648 experiment is kept separate from supplier ISO 75 results.
Read individual measurement and claim records
- polymaker htpla hdt 045 as printed temperature
- Temperature at the source ISO 75 deflection criterion under the stated flexural stress; not a continuous-use rating.: 61.4 °C. Supplier typical HDT: 61.4 °C, as printed, 0.45 MPa.
PDF p. 3, Thermal Properties, data row 7: Heat deflection temperature, ISO 75 0.45 MPa, as printed. Polymaker [details] - polymaker htpla hdt 045 annealed temperature
- Temperature at the source ISO 75 deflection criterion under the stated flexural stress; not a continuous-use rating.: 107.2 °C. Supplier typical HDT: 107.2 °C, annealed, 0.45 MPa.
PDF p. 3, Thermal Properties, data row 10: Heat deflection temperature, ISO 75 0.45 MPa, annealed. Polymaker [details] - polymaker htpla hdt 18 as printed temperature
- Temperature at the source ISO 75 deflection criterion under the stated flexural stress; not a continuous-use rating.: 58.6 °C. Supplier typical HDT: 58.6 °C, as printed, 1.8 MPa.
PDF p. 3, Thermal Properties, data row 6: Heat deflection temperature, ISO 75 1.8 MPa, as printed. Polymaker [details] - polymaker htpla hdt 18 annealed temperature
- Temperature at the source ISO 75 deflection criterion under the stated flexural stress; not a continuous-use rating.: 71.7 °C. Supplier typical HDT: 71.7 °C, annealed, 1.8 MPa.
PDF p. 3, Thermal Properties, data row 9: Heat deflection temperature, ISO 75 1.8 MPa, annealed. Polymaker [details] - hdt is load and time specific
- ISO 75 uses a heated three-point-bending test under defined stress. Its result does not establish maximum use temperature, design performance or long-term endurance.
Public Abstract §§1.1, 1.3 and 1.5. ISO [details] - hdt two stresses
- ISO 75-2 identifies 1.80 MPa for method A and 0.45 MPa for method B. They are different test stresses, not interchangeable HDT labels.
Public Abstract, methods A and B. ISO [details] - d648 is not iso75
- ASTM D648 limits extrapolation to other exposure conditions and says its results must not be compared with ISO 75-1/-2 results because their technical content differs.
Public Significance and Use §5.1; Scope Note 3. ASTM International [details] - vicat is penetration
- Vicat identifies a specified needle-penetration response during controlled heating, rather than the flexural deflection measured by HDT.
Public Scope §1.1; Significance and Use §§5.1–5.2. ASTM International [details] - tg by dsc
- DSC assigns a glass-transition temperature from a heat-capacity step in the material’s amorphous region.
Public Significance and Use §5.1; Scope §§1.1–1.2. ASTM International [details] - tg by dma
- DMA examines temperature- and frequency-dependent viscoelastic response. The glass transition spans a range; the reported assigned temperature depends on the technique.
Public Significance and Use §§5.2–5.3. ASTM International [details] - annealing changes printed pla
- The printed True Red PolyLite PLA study links thermal history, crystallinity and HDT. Its separately specified annealed specimens are not the HT-PLA grade or a transferable annealing recipe.
Experimental Section: Materials, Fused Deposition Modeling, Annealing and Thermal Analysis; Results: Dynamic Mechanical Analysis and Heat Deflection Temperature Changes, Figures 13–14. ACS Omega [details] - htpla annealing protocol gap
- The table labels annealed results; the recommendation and general recipe are separate from an identified HDT specimen protocol.
PDF p. 3, Thermal Properties; PDF p. 5, annealing note; PDF p. 6, How to Make Specimens. Polymaker [details] - prusa thermal basis gap
- The PC Blend sheet’s thermal rows are outside the explicitly printed mechanical table. Its tensile-coupon orientation and recipe are not established thermal-test conditions.
PDF p. 2, Typical material properties HDT rows, compared with the separate Mechanical properties of 3D printed testing specimens table and its footnote (3) on p. 3. Prusa Polymers a.s. [details] - creep below tg
- One printed Ultrafuse PLA specimen continued to creep under the long room-temperature bending hold below its glass transition. This evidence calls for a sustained-load check but does not supply a general lifetime prediction.
§3.1/Table 1 (material and process), §3.3 (test protocol), §4.2/Figure 11 and §5 (long-duration observations). Fischbach and Weinberg [details]